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A combination of cBCZ otherwise cgBCZ (1 mmol) and you may potassium tert-butoxide (168 milligrams, 1.5 mmol) have been demolished in the THF at the fifty °C, after which iodomethane (198 mg, step one.4 mmol) is added. Immediately after are cooled on the room-temperature, the new response mix try put to your CH2Cl2 (100 mL). The brand new natural covering are clean with h2o (50 mL) for three minutes, after which dried over Na2SO4. Pursuing the elimination of solvent below smaller tension, the fresh residue is actually purified by thumb chromatography for the silica serum so you can afford the target device cBCZ-Myself or cgBCZ-Myself. Fixed a bug you to definitely eliminated the player from lso are-going into the team an element of the fundamental battlefield “Slip of one’s Contaminated Eunuch” if the the specialist and you may Baishe was outdone from the the same go out.
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